Determination of Nicotine in Cigarette Tobacco Smuggled to Brazil by Modified QuEChERS Methodology

نویسندگان

چکیده

The study of cigarette authenticity in Brazil is important due to increasing consumption contraband cigarettes. Nicotine concentration an parameter reflecting the quality tobacco used production these Simple methods for this determination, which produce reduced waste, are environmentally and industrially important. nicotine smuggled was determined by QuEChERS method, requiring some modifications, such as decreasing volume extractor solvent, changes pH, removal sample hydration step. Quantification performed gas chromatography using a flame ionization detector. Doehlert matrix design optimize method. extraction recoveries ranged from 97.5% 99.6%, with relative standard deviation (RSD) ≤ 2.5% limits detection quantification 0.6 mg L-1 2.5 L-1, respectively. method sensitive accurate nicotine. cigarettes found be lower than that observed legal successfully applied real samples cigarettes, providing robust routine analysis proving need more studies on control Brazil.

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ژورنال

عنوان ژورنال: Orbital: The Electronic Journal of Chemistry

سال: 2022

ISSN: ['1984-6428']

DOI: https://doi.org/10.17807/orbital.v14i2.16188